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Beilstein J. Org. Chem. 2014, 10, 841–847, doi:10.3762/bjoc.10.80
Graphical Abstract
Figure 1: Columnar packing structures of buckybowls showing (a) unidirectional and (b) opposite structures, i...
Scheme 1: Synthesis of pyrenylsumanene (1): (a) Sc(OTf)3 (5 mol %), DIH (100 mol %), CH2Cl2, rt, 2.5 h, yield...
Figure 2: The X-ray crystal structure of 1, showing: (a) top view of the ORTEP drawing with 50% probability, ...
Figure 3: (a) Absorption spectra of 1, 3 and pyrene in CH2Cl2 solution (1.0 × 10−5 M); (b) emission spectra o...
Figure 4: Calculated HOMO and LUMO orbitals and HOMO–LUMO gaps (ΔE) for 1, 3 and pyrene (ωB97XD/6-31G(d)).